3,4,5-trimethoxy-N-3-pyridylbenzamide
Basic Information
- CAS No.: 31638-96-7
Physical properties
Product Description
Bulk supply high purity 3,4,5-trimethoxy-N-3-pyridylbenzamide 31638-96-7, Paid sample available
- Molecular Formula: C15H16 N2 O4
- Molecular Weight: 288.303
- Vapor Pressure: 1.84E-06mmHg at 25°C
- Boiling Point: 395.4°Cat760mmHg
- PKA: 11.91±0.70(Predicted)
- Flash Point: 192.9°C
- PSA： 73.17000
- Density: 1.234g/cm3
- LogP: 2.74370
3,4,5-trimethoxy-N-3-pyridylbenzamide(Cas 31638-96-7) Usage
InChI:InChI=1/C15H16N2O4/c1-19-12-7-10(8-13(20-2)14(12)21-3)15(18)17-11-5-4-6-16-9-11/h4-9H,1-3H3,(H,17,18)
31638-96-7 Relevant articles
A mesoionic nitrogen-donor ligand: Structure, iridium coordination, and catalytic effects
Navarro, Miquel,Li, Mo,Bernhard, Stefan,Albrecht, Martin
, p. 659 - 662 (2017)
A mesoinic pyridylideneamide ligand (PYA...
Troxipide preparation method
-
Paragraph 7; 8, (2019/02/27)
The invention belongs to the field of ph...
31638-96-7 Process route
-
-
462-08-8
pyridin-3-ylamine
-
-
4521-61-3
3,4,5-Trimethoxybenzoyl chloride
-
-
31638-96-7
3,4,5-trimethoxy-N-3-pyridylbenzamide
| Conditions | Yield |
|---|---|
|
With
sodium carbonate;
In
dichloromethane;
at 40 ℃;
for 4h;
Temperature;
Reagent/catalyst;
Solvent;
|
86.2%
|
|
With
triethylamine;
In
tetrahydrofuran;
at 20 ℃;
for 18h;
|
85%
|
-
-
118-41-2
Eudesmic acid
-
-
31638-96-7
3,4,5-trimethoxy-N-3-pyridylbenzamide
| Conditions | Yield |
|---|---|
|
Multi-step reaction
with
2
steps
1: bis(trichloromethyl) carbonate / dichloromethane; N,N-dimethyl acetamide / 3 h / 30 °C
2: sodium carbonate / dichloromethane / 4 h / 40 °C
With
bis(trichloromethyl) carbonate; sodium carbonate;
In
dichloromethane; N,N-dimethyl acetamide;
|
31638-96-7 Upstream products
-
462-08-8
pyridin-3-ylamine
-
4521-61-3
3,4,5-Trimethoxybenzoyl chloride
-
118-41-2
Eudesmic acid
31638-96-7 Downstream products
-
30751-05-4
troxipide